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Beilstein J. Org. Chem. 2014, 10, 814–824, doi:10.3762/bjoc.10.77
Graphical Abstract
Scheme 1: Off- (open) and on- (closed) states of a ditopic positive allosteric receptor based on a 4,4’-funct...
Scheme 2: Bis(β-cyclodextrin)-functionalised 2,2’-bipyridines 1–3.
Scheme 3: Synthesis of diisothiocyanato-2,2’-bipyridines 14–16.
Scheme 4: Synthesis of peracetylated cyclodextrin 21.
Scheme 5: Synthesis of receptors 1–3.
Figure 1: X-ray crystal structure analysis of [(CO)3Re(14)Cl] (colour code: petrol: rhenium, grey: carbon, re...
Figure 2: MALDI mass spectrum (sample prepared from a 1:1 mixture of CuPF6 and 2 in benzene/acetonitrile (1:1...
Figure 3: Aromatic region of the 1H NMR spectra (400.1 MHz, 293 K, benzene-d6/acetonitrile-d3 1:1) of a) 1 an...
Figure 4: Aromatic region of the 1H NMR spectra (400.1 MHz, 293 K, benzene-d6/acetonitrile-d3 1:1) of a) 2 an...
Scheme 6: Synthesis of ligand 22.
Figure 5: X-ray crystal structure analysis of [Cu(H3CCN)2(22)]BF4 and [Zn(22)2](OTf)2 (counterions are omitte...
Figure 6: Aromatic region of the 1H NMR spectra (400.1 MHz, 293 K, benzene-d6/acetonitrile-d3 1:1) of a) 1, b...
Figure 7: MALDI–TOF mass spectrum (sample prepared from of a 1:1:1 mixture of CuPF6, 22, and 1 in benzene/ace...